R & D innovation
Center Introduction
Our company's R&D center was officially established in 2012. In 2020, the R&D institution was approved as the Hubei Provincial Joint Innovation Center for Fine Phosphorus Chemicals and New Materials between enterprises and schools, and in 2020, the Hubei Provincial Enterprise Technology Center was established to further deepen the cooperation between industry, academia, and research. The company has built a dedicated R&D center building, covering an area of approximately 1860 square meters, which has become a technical institution integrating scientific research, production, and development, specifically engaged in the development and application of new products and new technologies, and actively carries out international and domestic exchanges and cooperation. During the process of undertaking technological innovation projects, the R&D center continuously optimizes the functions of internal departments, enriches departmental functions, and accumulates a strong technical foundation through team expansion, new equipment addition, and increased investment. It has transformed from an initially functionally single R&D department into a key institution that has established and implemented a comprehensive technological innovation system, with sub-departments including the Development Department, Design Office, Process Department, Quality Supervision Center, and Safety Energy and Environmental Protection Department. It is capable of formulating the company's innovation plan, carrying out industrial technology R&D, creating and utilizing intellectual property, establishing a technical standard system, cultivating innovative talents, building a collaborative innovation network, and promoting the implementation of the entire process of technological innovation. Currently, the technology center has a total of 72 technical personnel, accounting for 23% of the total number of employees, with 40 technical personnel holding a bachelor's degree or above, and 38 technical personnel at the intermediate level or above.
Achievement Transformation
Our company has accumulated 42 patents, including 9 invention patents. The R&D results have achieved good technology transfer. The "two-step method" process for producing Phosphoric Acid and the efficient air-cooled continuous crystallization process for producing Phosphoric Acid diammonium hydrogen phosphate are the first of their kind in the country. They address shortcomings, fill gaps, reduce energy consumption, promote the green development of the phosphorus chemical industry chain, and enhance the international competitiveness of our Phosphoric Acid salt products. The high-purity electronic-grade Phosphoric Acid produced using new melt crystallization technology meets the requirements of the International Semiconductor Materials Committee (SEMI) and has been recognized by domestic and foreign users, breaking the long-standing import situation. The precursor series products of Ammonium Phosphate, developed over many years for the positive electrode materials of new energy power batteries, have won users' favor with their innovative technology and first-class quality, becoming the largest supplier of raw materials for domestic new energy power battery positive electrode materials. We have become the production and sales base for fine Phosphoric Acid salts in China and a pillar enterprise in the subdivided field in Hubei Province.
Talent cultivation
(1) Recruiting and cultivating high-end talents, continuously optimizing the talent structure, and gradually increasing the proportion of high-ranking personnel have provided strong talent support for the innovative development of the R&D center. By utilizing internal referrals, social recruitment, and other channels, and leveraging a comprehensive salary standard and promotion space, we attract technical talents from the industry. At the same time, we focus on improving the technical level of internal technical personnel, with 15 new mid-level title personnel and 2 junior title technical personnel trained in the past three years.
(2) Hiring senior expert professors to further enhance the research strength and influence of the R&D center. We have carried out multiple technical collaborations around the production technology of fine phosphor industrial products, hydrogen peroxide and peroxide production technology, etc., promoting the research of new products and new technologies, and facilitating the successful implementation of research projects.
(3) Conducting internal training and further education to enhance employees' professional skills and knowledge levels. By formulating targeted talent training plans, clarifying training objectives, content, and methods, we promote the stable development of the talent team, enhance team collaboration and communication, stimulate innovative thinking and creativity, and optimize the talent structure and echelon construction, improving the relevance and effectiveness of performance assessments. In the past three years, we have promoted 15 technical backbones, held over 30 internal training exchange meetings, and conducted more than 10 external training sessions, including high-quality development training courses for the petrochemical industry in Wuhan, safety production knowledge and management capability assessment training, and special operations supervisor qualification training, enhancing the research level of the innovation team and the safety production capability of hazardous chemicals.
Representative Projects
Research on the Preparation Method of Flame Retardant Phosphoric Acid Dihydrogen Potassium Granules
Key Technologies and Innovations:
(1) Using an atomization method instead of a dropwise addition method to introduce raw materials, controlling the reaction process and system stability, suppressing side reactions and the generation of impurities. Optimizing the reaction process, eliminating the need for concentration crystallization steps, and improving the performance of Phosphoric Acid Dihydrogen Potassium through coating modification reactions. A process technology that couples mist-liquid interface reactions and dual neutralization reactions.
(2) The preparation process of Phosphoric Acid Dihydrogen Potassium optimizes the traditional neutralization method, effectively improving product quality and reducing production costs, thus opening up a product granule that meets flame retardant requirements without crystallization steps, effectively reducing energy consumption and eliminating waste liquid discharge.
Research and Development of Low-Arsenic Polyphosphoric Acid and Phosphoric Acid Salts
Key Technologies and Innovations:
(1) By using a Phosphoric Acid arsenic removal system, the amount of arsenic removal agent is reduced, resulting in low arsenic content and high-quality products of polyphosphoric acid and phosphoric acid salts.
(2) Utilizing a thermal method phosphoric acid reaction tower can recover more than 50% of the combustion heat of yellow phosphorus and can produce 0.8 to 3.8 MPa steam as a byproduct. This solves the heat required in the process flow, achieving the goals of saving coal and water resources, conserving energy, and reducing production costs, thereby achieving energy conservation and emission reduction from the source of the process.
(3) Achieving metering and adjustment of yellow phosphorus and polyphosphoric acid through an electromagnetic flow meter and a frequency adjustment system, using an automatic display instrument that integrates density, temperature, and flow to control the density adjustment of polyphosphoric acid, facilitating automatic detection and control of key process parameters.
Research and Development of High I-Type Food Grade Polyphosphoric Acid Salts
Key Technologies and Innovations:
(1) High-temperature hot air obtained from burning natural gas is mixed with combustion air supplied by an air blower in the polymerization furnace burner for uniform combustion, providing a drying polymerization heat source, making the polycondensation reaction of phosphoric acid salts faster and more complete.
(2) Fine-tuning the neutralization degree, polymerization degree, and tail temperature control of the polymerization furnace to enhance the sodium pentavalent content and polymerization effect, while reducing the content of insoluble substances in water.
(3) Effectively controlling the reaction temperature in the polymerization furnace and the partial pressure of water vapor in the reaction environment, increasing the content of sodium pentavalent type I.
(4) Optimizing the raw materials for food-grade polyphosphoric acid salts:
Self-produced food additive phosphoric acid, colorless and transparent in appearance, with a content of ≧75%;
Sodium carbonate arsenic content (as As) ≤3ppm, heavy metals (as Pb) ≤10ppm;
Liquid sodium hydroxide arsenic content (as As) ≤3pp, heavy metals (as Pb) ≤10ppm.
Research on the Preparation Method of Electronic Grade Phosphoric Acid
Key Technologies and Innovations:
(1) By regulating the reaction temperature, pressure, and time, optimizing the thermal method phosphoric acid preparation process, reducing the generation of metal ions, and lowering the metal ion content in phosphoric acid to the ppm level, significantly enhancing the purity of phosphoric acid.
(2) Integrating various technologies such as crystallization purification, ion exchange, adsorption, and membrane separation to achieve efficient removal of impurities such as metal ions in phosphoric acid, while reducing the introduction of impurities and improving the quality of phosphoric acid.
(3) Establishing an online monitoring system for product quality to detect key indicators such as metal ion content in phosphoric acid in real-time, optimizing the production process through feedback control, and ensuring the stability of product quality.
Research and Development Strength
In the past three years, our company's technological innovation has achieved rich scientific and technological innovation results, and the overall technical level is at the leading level in the industry. We have newly applied for 18 patents, including 7 invention patents and 11 utility model patents. We have newly authorized 15 patents, including 5 invention patents (3 jointly applied with Wuhan University of Engineering) and 10 utility model patents, further improving production efficiency, reducing production costs, enhancing product quality, and increasing the market competitiveness of our products.